CRYSTALLINITY PREDICTION OF SHORT CARBON FIBRE REINFORCED POLYAMIDE 6 COMPOSITES MANUFACTURED BY FUSED FILAMENT FABRICATION

Yifan Zhu; Lenny Van Daele; Sandra Van Vlierberghe; Lincy Pyl

doi:10.5075/epfl-298799_978-2-9701614-0-0

CRYSTALLINITY PREDICTION OF SHORT CARBON FIBRE REINFORCED POLYAMIDE 6 COMPOSITES MANUFACTURED BY FUSED FILAMENT FABRICATION

Yifan Zhu, Lenny Van Daele, Sandra Van Vlierberghe, Lincy Pyl

Research output: Chapter in Book/Report/Conference proceeding › Conference paper

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Abstract

Polymer additive manufacturing has transformed itself from a technology that is mainly focused on rapid prototyping to a widely received manufacturing technique for highly customised products. In fused filament fabrication (FFF), due to the fast heating and cooling of the polymer, the printed part's crystallinity and mechanical properties are inevitably affected. This research proposes a numerical approach to predict the final crystallinity for FFF printed polyamide 6/short carbon fibre composite. To do so, samples were built with the FFF technique with their temperature history recorded by infrared camera measurements. Differential scanning calorimetry (DSC) was conducted on the FFF filament to calibrate the numerical model. Temperature history was used as input for the model and the printed part’s final crystallinity is predicted. Tensile tests were carried out to examine the influence of crystallinity on the printed part’s mechanical performance.

Original language	English
Title of host publication	CRYSTALLINITY PREDICTION OF SHORT CARBON FIBRE REINFORCED POLYAMIDE 6 COMPOSITES MANUFACTURED BY FUSED FILAMENT FABRICATION
Editors	Anastasios P. Vassilopoulos, Veronique Michaud
Place of Publication	Proceedings of the 20th European Conference on Composite Materials - Composites Meet Sustainability
Publisher	EPFL Lausanne, Composite Construction Laboratory
Pages	399-406
Number of pages	8
Volume	2
ISBN (Electronic)	978-2-9701614-0-0
DOIs	https://doi.org/10.5075/epfl-298799_978-2-9701614-0-0
Publication status	Published - 12 Dec 2022

Publication series

Name	ECCM 2022 - Proceedings of the 20th European Conference on Composite Materials: Composites Meet Sustainability
Volume	2

Bibliographical note

Funding Information:
The authors gratefully acknowledge the support from Department for Economy (DfE) for funding the project.

Funding Information:
The authors acknowledge the support of the Agency for Innovation and Entrepreneurship Flanders via the Strategic Initiative Materials in Flanders in the framework of the SIM-SBO PET2VALUE project, running in the NANOFORCE program.

Publisher Copyright:
© 2022 Zhu et al.

Copyright:
Copyright 2023 Elsevier B.V., All rights reserved.

Keywords

Fused filament fabrication
Short fibre reinforced thermoplastic
Crystallinity

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10.5075/epfl-298799_978-2-9701614-0-0

CRYSTALLINITY PREDICTION OF SHORT CARBON FIBRE REINFORCED POLYAMIDE 6 COMPOSITES MANUFACTURED BY FUSED FILAMENT FABRICATIONAccepted author manuscript, 439 KB

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Zhu, Y., Van Daele, L., Van Vlierberghe, S., & Pyl, L. (2022). CRYSTALLINITY PREDICTION OF SHORT CARBON FIBRE REINFORCED POLYAMIDE 6 COMPOSITES MANUFACTURED BY FUSED FILAMENT FABRICATION. In A. P. Vassilopoulos, & V. Michaud (Eds.), CRYSTALLINITY PREDICTION OF SHORT CARBON FIBRE REINFORCED POLYAMIDE 6 COMPOSITES MANUFACTURED BY FUSED FILAMENT FABRICATION (Vol. 2, pp. 399-406). (ECCM 2022 - Proceedings of the 20th European Conference on Composite Materials: Composites Meet Sustainability; Vol. 2). EPFL Lausanne, Composite Construction Laboratory. https://doi.org/10.5075/epfl-298799_978-2-9701614-0-0

Zhu, Yifan ; Van Daele, Lenny ; Van Vlierberghe, Sandra et al. / CRYSTALLINITY PREDICTION OF SHORT CARBON FIBRE REINFORCED POLYAMIDE 6 COMPOSITES MANUFACTURED BY FUSED FILAMENT FABRICATION. CRYSTALLINITY PREDICTION OF SHORT CARBON FIBRE REINFORCED POLYAMIDE 6 COMPOSITES MANUFACTURED BY FUSED FILAMENT FABRICATION. editor / Anastasios P. Vassilopoulos ; Veronique Michaud. Vol. 2 Proceedings of the 20th European Conference on Composite Materials - Composites Meet Sustainability : EPFL Lausanne, Composite Construction Laboratory, 2022. pp. 399-406 (ECCM 2022 - Proceedings of the 20th European Conference on Composite Materials: Composites Meet Sustainability).

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abstract = "Polymer additive manufacturing has transformed itself from a technology that is mainly focused on rapid prototyping to a widely received manufacturing technique for highly customised products. In fused filament fabrication (FFF), due to the fast heating and cooling of the polymer, the printed part's crystallinity and mechanical properties are inevitably affected. This research proposes a numerical approach to predict the final crystallinity for FFF printed polyamide 6/short carbon fibre composite. To do so, samples were built with the FFF technique with their temperature history recorded by infrared camera measurements. Differential scanning calorimetry (DSC) was conducted on the FFF filament to calibrate the numerical model. Temperature history was used as input for the model and the printed part{\textquoteright}s final crystallinity is predicted. Tensile tests were carried out to examine the influence of crystallinity on the printed part{\textquoteright}s mechanical performance.",

keywords = "Fused filament fabrication, Short fibre reinforced thermoplastic, Crystallinity",

author = "Yifan Zhu and {Van Daele}, Lenny and {Van Vlierberghe}, Sandra and Lincy Pyl",

note = "Funding Information: The authors gratefully acknowledge the support from Department for Economy (DfE) for funding the project. Funding Information: The authors acknowledge the support of the Agency for Innovation and Entrepreneurship Flanders via the Strategic Initiative Materials in Flanders in the framework of the SIM-SBO PET2VALUE project, running in the NANOFORCE program. Publisher Copyright: {\textcopyright} 2022 Zhu et al. Copyright: Copyright 2023 Elsevier B.V., All rights reserved.",

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Zhu, Y, Van Daele, L, Van Vlierberghe, S & Pyl, L 2022, CRYSTALLINITY PREDICTION OF SHORT CARBON FIBRE REINFORCED POLYAMIDE 6 COMPOSITES MANUFACTURED BY FUSED FILAMENT FABRICATION. in AP Vassilopoulos & V Michaud (eds), CRYSTALLINITY PREDICTION OF SHORT CARBON FIBRE REINFORCED POLYAMIDE 6 COMPOSITES MANUFACTURED BY FUSED FILAMENT FABRICATION. vol. 2, ECCM 2022 - Proceedings of the 20th European Conference on Composite Materials: Composites Meet Sustainability, vol. 2, EPFL Lausanne, Composite Construction Laboratory, Proceedings of the 20th European Conference on Composite Materials - Composites Meet Sustainability, pp. 399-406. https://doi.org/10.5075/epfl-298799_978-2-9701614-0-0

CRYSTALLINITY PREDICTION OF SHORT CARBON FIBRE REINFORCED POLYAMIDE 6 COMPOSITES MANUFACTURED BY FUSED FILAMENT FABRICATION. / Zhu, Yifan; Van Daele, Lenny; Van Vlierberghe, Sandra et al.
CRYSTALLINITY PREDICTION OF SHORT CARBON FIBRE REINFORCED POLYAMIDE 6 COMPOSITES MANUFACTURED BY FUSED FILAMENT FABRICATION. ed. / Anastasios P. Vassilopoulos; Veronique Michaud. Vol. 2 Proceedings of the 20th European Conference on Composite Materials - Composites Meet Sustainability: EPFL Lausanne, Composite Construction Laboratory, 2022. p. 399-406 (ECCM 2022 - Proceedings of the 20th European Conference on Composite Materials: Composites Meet Sustainability; Vol. 2).

Research output: Chapter in Book/Report/Conference proceeding › Conference paper

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AU - Van Vlierberghe, Sandra

AU - Pyl, Lincy

N1 - Funding Information: The authors gratefully acknowledge the support from Department for Economy (DfE) for funding the project. Funding Information: The authors acknowledge the support of the Agency for Innovation and Entrepreneurship Flanders via the Strategic Initiative Materials in Flanders in the framework of the SIM-SBO PET2VALUE project, running in the NANOFORCE program. Publisher Copyright: © 2022 Zhu et al. Copyright: Copyright 2023 Elsevier B.V., All rights reserved.

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N2 - Polymer additive manufacturing has transformed itself from a technology that is mainly focused on rapid prototyping to a widely received manufacturing technique for highly customised products. In fused filament fabrication (FFF), due to the fast heating and cooling of the polymer, the printed part's crystallinity and mechanical properties are inevitably affected. This research proposes a numerical approach to predict the final crystallinity for FFF printed polyamide 6/short carbon fibre composite. To do so, samples were built with the FFF technique with their temperature history recorded by infrared camera measurements. Differential scanning calorimetry (DSC) was conducted on the FFF filament to calibrate the numerical model. Temperature history was used as input for the model and the printed part’s final crystallinity is predicted. Tensile tests were carried out to examine the influence of crystallinity on the printed part’s mechanical performance.

AB - Polymer additive manufacturing has transformed itself from a technology that is mainly focused on rapid prototyping to a widely received manufacturing technique for highly customised products. In fused filament fabrication (FFF), due to the fast heating and cooling of the polymer, the printed part's crystallinity and mechanical properties are inevitably affected. This research proposes a numerical approach to predict the final crystallinity for FFF printed polyamide 6/short carbon fibre composite. To do so, samples were built with the FFF technique with their temperature history recorded by infrared camera measurements. Differential scanning calorimetry (DSC) was conducted on the FFF filament to calibrate the numerical model. Temperature history was used as input for the model and the printed part’s final crystallinity is predicted. Tensile tests were carried out to examine the influence of crystallinity on the printed part’s mechanical performance.

KW - Fused filament fabrication

KW - Short fibre reinforced thermoplastic

KW - Crystallinity

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DO - 10.5075/epfl-298799_978-2-9701614-0-0

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BT - CRYSTALLINITY PREDICTION OF SHORT CARBON FIBRE REINFORCED POLYAMIDE 6 COMPOSITES MANUFACTURED BY FUSED FILAMENT FABRICATION

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PB - EPFL Lausanne, Composite Construction Laboratory

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Zhu Y, Van Daele L, Van Vlierberghe S, Pyl L. CRYSTALLINITY PREDICTION OF SHORT CARBON FIBRE REINFORCED POLYAMIDE 6 COMPOSITES MANUFACTURED BY FUSED FILAMENT FABRICATION. In Vassilopoulos AP, Michaud V, editors, CRYSTALLINITY PREDICTION OF SHORT CARBON FIBRE REINFORCED POLYAMIDE 6 COMPOSITES MANUFACTURED BY FUSED FILAMENT FABRICATION. Vol. 2. Proceedings of the 20th European Conference on Composite Materials - Composites Meet Sustainability: EPFL Lausanne, Composite Construction Laboratory. 2022. p. 399-406. (ECCM 2022 - Proceedings of the 20th European Conference on Composite Materials: Composites Meet Sustainability). doi: 10.5075/epfl-298799_978-2-9701614-0-0

CRYSTALLINITY PREDICTION OF SHORT CARBON FIBRE REINFORCED POLYAMIDE 6 COMPOSITES MANUFACTURED BY FUSED FILAMENT FABRICATION

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